One of the major challenges in creatingextremelywell-organized nanostructure photo electrodes are to attainbettermanaging toolfor the specified morphology and enhances electrical conductivity. We create ahighly well-organized plasma-processing method to form uniform porous structures in tin as substrates. The tin oxide based Nano formulations were experimentally characterized for encapsulation potential power, particle size distribution, morphology of nanoparticles, zeta potential for stability, FTIR, and uniform entrapment. It was experimentally found that Nano formulations possessed particle size within the range of 122-290 nm and having a good encapsulation efficiency of 90-93%. These research outcomes suggested that tin oxide based nanoparticles as advance mesoporous tin oxide layering system. After performing optimizationof forming Nano composite,performed procedure of annealing, the mesoporous tin transforms into photoactive monoclinic SnO2. The exceptional positive control over the Nano composite size and strong contact force created between the crystallites obtained through plasma method offers astimulatingnovel synthesis method for Nano composite resources for use in various processes like solar energy dependent water splitting.